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Ni基体磁控溅射离子镀Al膜的电镜观察

万立骏 , 陈宝清 , 郭可信

金属学报

利用横截面电镜样品,对Ni基体磁控溅射离子镀Al膜进行了透射电镜观察。研究了不同工艺条件下镀膜的组织形态,相结构以及相分布。镀覆5min时,在Ni基体和镀Al膜交界处,发现一个Al-Ni系中迄今未见报道的未知相。经电子衍射分析其为体心四方点阵,a=b=0.588nm,c=0.480nm。研究了随时间变化的镀膜组织结构变化情况。

关键词: 磁控溅射 , ion-plating , microstructure , plated film

TEM OBSERVATION OF ION-PLATED Al FILM ON Ni SUBSTRATE

WAN Lijun Dalian Maritime University , Dalian , Liaoning , China CHEN Baoqing Dalian Institute of Technology , Dalian , Liaoning , China GUO Kexin(K.H.KUO) Institute of Metal Research , Academia Sinica , Shenyang , China Institute of Metal and Technology , Dalian Maritime University , Dalian , Liaoning , China

金属学报(英文版)

A new phase was found at the interface between Al film and Ni substrate when the time of ion-plating reaches 5 min.It was identified to be body centered tetragonal lattice with the constants a=b=0.588 nm,c=0.480 nm.The variation of microstructure and phases with the ion-plating time were observed.Based on these results,the ion-plating film formation mech- anism has been also discussed.

关键词: magnetron sputtering , null , null , null

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